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UNK39.TXT
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1993-02-13
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4KB
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202 lines
The solid was insoluble in the usual reagents.
1348
Typical of a saturated or aromatic hydrocarbon or a halogenated compound.
Solvent is deuterochloroform.
τµµτσσττµµµσσµτµσµτµµµµµµσσσσσµµµµµµµµµµµµµµµσµµµµτττµσσσΣΣΣΣΣσµµσµµµµµµµµµσσµΣππΓß▀▄╒╒h 3j▐ΣµΓΓσττττττττµµττττττµµσσσσσσσσµτµσµµµµτµµµµτττµµτττττττΦτµµµττττΦΦΦττττµµµµσσµµµττµσσµµτµµµττττττττττττµµµµµµτττττττττσµµµµµτµµττµµσσµµµµµµµσµσσσµσσσσσΣΣΣΣσσσµµµµ
µττττµσσµσσµµµµµσµµµµµµµµµµµµµµµµµµµττττµµτµτµµσσΣσµσσΣπσµµτττττττττττΦτττττµτττµµµττττττττττµµσστµσσττττττµµµµµµττττττµµττµµµµµµτµµµµµττµσµµµµττττττττττττττττττµτττττµµτττττττττττττττττττµττΦττττττΦΦΦτττττττττττΦτµµµµµµττττττττττττττµµµµµττττττττττµττττµ
µΣΣΣσµτττµµττµµµµτττΦΦΦΦΦττΦτττττττΦΦΦΦΦΦΦΦτΦΦΦττττττττττττττττµτΦτττττττττττττττττµτττττττµµµµσΣπΓ▐╪┘▀πσµµττττΦΦΦΦΦ
132023303334383941424344454648495154
Only aromatic protons, all of one type, are present.
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dummy ms
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Bromine was found to be present.
21253135394142434948
Absent are nitrogen and sulfur.
No residue was left after burning (with a sooty flame).
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The compound is not a metal salt but is aromatic or unsaturated.
87 to 89 degrees.
#
A low melting solid.
Nujol mull
+*-+)((()())'))(()**)(()')+)))*)(()+*()))*+*+++,,,--....//////000001122344567789:<=?@IMGJMST`h~ƒ└╓┘▀ΣΦ╓╟│╜╞┼ºÇk4*&$#$%+*+,-,+-/-...-,++**+)((''''''''((())))*,**+*,02/,,++,-----,*))))))))))**))))*****++,+++++++++1AMH220--.///////////00002464358665333333334
433332337BI?87664444443332222222;B_XNFQÜσ╓╣ƒ~qaQHBBFOHNZoòª{`XONPKFDDDEFDCBAA@>OVMB=<<<?A;98888889988678??82.9FK/@_cI@£▓]RLE>84,6v¼╩═v_VPMKIHVICB@=;;;;;;:;:76688789;=H╜ΓáqSID@=<;;?@?@CGJC8Z5/+)''&'&'*%$&"!#%$$! " '&'%)'"#&%))3Iº\>?=BBJréYT\\TC
1419222427294231531320233033343839414243444546484951542850
Shows the presence of aromaticity and absence of many functional groups.
217-219 degrees.
#
Typical value for a liquid.
Optically inactive.
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The compound is achiral.
Not usually measured for a solid.
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Mainly for liquids.
Not usually measured for a solid.
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Usually measured only for liquids.
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dummy cmr
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No precipitate was formed.
2227282950
The unknown is not a ketone or aldehyde.
No positive result.
3344454651
The compound does not contain any reactive hydrogens ie: OH, NH, SH.
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No reaction took place.
14
The commpound is not an ester.
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No reaction was observed.
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The halogen is not reactive ( ie tertiary or aromatic).
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No positive result.
3344454651
Absent are OH (alcohol or phenol) and NH (prim. or sec. amine) containing groups
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No change was observed.
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The compound is not easily oxidizable.
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No colour change was observed.
232850
The unknown is not a sugar.
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No visible change was noted.
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The unknown is not a phenol nor is it unsaturated.
No reaction took place.
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Ether groups are absent.
No reaction.
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The compound is not a phenol.
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No precipitate formed even after heating.
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No reaction; typical of aromatic compounds.
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A solution was formed.
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This is typical of an aromatic hydrocarbon.
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No reaction observed.
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The unknown is not a phenol nor is it unsaturated.
No reaction.
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The compound is not a ester, acetal, amide or a nitrile.
No positive result.
3344454651
Absent are groups containing OH (ROH or ArOH) or NH (prim. or sec. amine).
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colourless crystalline solid
010507
2640
6395
Colourless solid m.p. 194-197 degrees.
Crystals m.p. range 80 to 84 degrees.
2
ª¥¬╣ó║o¡┴_ë╕╢ª┐╖
ç£Ü¥ñ▒b▓┴jô¼í»╦╖k¬
solid bromine containing compound
2
1,4-dibromonaphthalene
1,4-dibromobenzene